白屈菜蜜炙工艺的优化
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篇名: 白屈菜蜜炙工艺的优化
TITLE: Optimization of the Honey-stir-fired Technology of Chelidonium majus
摘要: 目的:优化白屈菜的蜜炙工艺。方法∶以水与炼蜜质量比、蜜水与白屈菜质量比、炒制温度、炒制时间为考察因素,白屈菜碱、盐酸黄连碱、血根碱、小檗碱、白屈菜红碱总含量为响应值,采用Box-Behnken响应面法优化其蜜炙工艺并验证。结果:最优蜜炙工艺为水与炼蜜质量比1∶1.9(g/g),蜜水与白屈菜质量比21∶100(g/g),炒制温度122℃,炒制时间10.40min。经3次试验验证,5种成分的平均总含量为10.37mg/g,RSD为0.23%,与预测值(10.39mg/g)的相对误差为0.19%。结论:优化所得白屈菜蜜炙工艺稳定、可行。
ABSTRACT: OBJECTIVE:To optimize the honey-stir-fried technology of Chelidonium majus . METHODS :Taking the mass ratio of water to honey ,the ratio of honey water to C. majus ,stir-fired temperature ,stir-fired time as the factors ,the total contents of chelidonine ,coptisine hydrochloride ,sanguinarine,berberine,chelerythrine as response values ,Box-Behnken response surface method was used to optimize the processing technology ,and valifation test was conducted. RESULTS :The optimum process conditions were as follows the ratio of water to refined honey 1∶1.9(g/g),the ratio of honey water to C. majus 21∶100(g/g), stir-fried temperature 122 ℃,stir-fried time 10.40 min. After 3 times of validation ,average total contents of 5 components was 10.37 mg/g(RSD=0.23%),relative error of which with predicted value (10.39 mg/g)was 0.19%. CONCLUSIONS :The optimized honey-stir-fried technology of C. majus is stable and feasible.
期刊: 2021年第32卷第12期
作者: 王仁广,隋欣彤,汪艳群,王鑫荣,钟修俊,赵天倚,王淑敏
AUTHORS: WANG Renguang, SUI Xintong,WANG Yanqun,WANG Xinrong,ZHONG Xiujun,ZHAO Tianyi,WANG Shumin
关键字: 白屈菜;蜜炙工艺;Box-Behnken响应面法;含量测定
KEYWORDS: Chelidonium majus ;Honey-stir-fried technology ;Box-Behnken response surface method ;Content determination
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