目的：建立复方金芩片的质量标准。方法：采用薄层色谱（TLC）法对制剂中黄柏、金银花进行定性鉴别。采用高效液相

色谱法测定制剂中黄芩苷的含量：色谱柱为Zorbax Eclipse XDB-C18，流动相为甲醇-0.2％磷酸（40 ∶60，V/V），流速为1.0 ml/min，检

测波长为280 nm，柱温为35 ℃，进样量为10 μl。结果：黄柏、金银花的TLC图斑点清晰，分离度好。黄芩苷检测进样量线性范围

为0.533～4.264 μg（r＝0.999 9）；精密度、稳定性、重复性试验的RSD＜2％；加样回收率为96.95％～99.70％（RSD＝1.18％，n＝

6）。结论：所建标准可用于复方金芩片的质量控制。

OBJECTIVE：To establish the quality standard of Fufang jinqin tablet. METHODS：TLC was conducted for the qualitative

identification of Cortex phellodendri and Lonicera japonica in the preparation. And HPLC was conducted for the content determination

of baicalin；the column was Zorbax Eclipse XDB-C18 with mobile phase of methanol-0.2％ phosphoric acid water（40 ∶

60，V/V）at a flow rate of 1.0 ml/min，the detection wavelength was 280 nm，column temperature was 35 ℃，and the injection volume

of 10 μl. RESULTS：C. phellodendri and L. japonica of TLC showed clear spots and good separation. The linear range of baicalin

was 0.533-4.264 μg（r＝0.999 9）；RSDs of precision，stability and reproducibility tests were lower than 2％；recovery was

96.95％-99.70％（RSD＝1.18％，n＝6）. CONCLUSIONS：The standard can be used for the quality control of Fufang jinqin tablet.